【药物名称】Indisulam, E-7070, ER-35744
化学结构式(Chemical Structure):
参考文献No.26532
标题:Bicyclic heterocyclic sulfonamide and sulfonic ester derivs.
作者:Yoshino, H.; Yamato, T.; Okauchi, T.; Yoshimatsu, K.; Sugi, N.; Nagasu, T.; Ozawa, Y.; Koyanagi, N.; Kito, K. (Eisai Co., Ltd.)
来源:EP 0673937; US 5721246; WO 9507276
合成路线图解说明:

The reaction of 7-nitro-1H-indole (I) with NCS in acetonitrile gives 3-chloro-7-nitro-1H-indole (II), which is reduced with Fe and NH4Cl or stannous chloride in ethanol/aq. HCl to yield 3-chloro-1H-indol-7-amine (III). Finally, this compound is condensed with 4-sulfamoylbenzenesulfonyl chloride (IV) in pyridine to afford the target sulfonamide. The intermediate 4-sulfamoylbenzenesulfonyl chloride (IV) is obtained by diazotation of 4-aminobenzenesulfonamide (V) with NaNo2 and HCl, followed by treatment with SO2 and CuCl2.

Drug Information Express,Drug R&D,Chemical Database,Patent Search.
Copyright © 2006-2024 Drug Future. All rights reserved.Contact Us