【药物名称】BAY-36-7620
化学结构式(Chemical Structure):
参考文献No.40029
标题:Substd. alpha,beta-anellated butyrolactones
作者:Horv醫h, E.; De Vry, J.-M.-V.; Baumgarten, J.; Schreiber, R.; Lensky, S.; M黮ler, T.; Stropp, U.; Voerste, A.; M黮ler, G.; Antonicek, H.-P.; Stolle, A.; Von dem Bruch, K. (Bayer AG)
来源:DE 19801646; EP 1047684; WO 9936416
合成路线图解说明:

The previously reported chiral cyclopentanedicarboxylic acid monoester (I) was converted to the mixed anhydride (II) by treatment with ethyl chloroformate in the presence of triethylamine. Reduction of the mixed anhydride (II) with NaBH4 in cold MeOH produced the corresponding alcohol, which, under the reaction conditions, gave rise to the bicyclic lactone (III). Then, the lithium enolate generated from lactone (III) and lithium hexamethyldisilazide was alkylated with 2-(bromomethyl)naphthalene (IV) to produce the title compound.

Drug Information Express,Drug R&D,Chemical Database,Patent Search.
Copyright © 2006-2024 Drug Future. All rights reserved.Contact Us