【药物名称】
化学结构式(Chemical Structure):
参考文献No.565106
标题:A new benzoangelicin with strong photobiological activity
作者:Santana, L.; Uriarte, E.; Dalla Via, L.; Gia, O.
来源:Bioorg Med Chem Lett 2000,10(2),135
合成路线图解说明:

Condensation of 7-hydroxy-5-methoxy-4-methylcoumarin (I) with 2-chlorocyclohexanone (II) by means of K2CO3 in refluxing acetone affords derivative (III), which is then cyclized by means of refluxing NaOH to provide compound (IV). Oxidation of (IV) by means of DDQ in refluxing benzene furnishes angelicine (V), whose methoxy group is then hydrolyzed with HI and acetic anhydride in refluxing HOAc to yield compound (VI). Finally, the desired product is obtained by coupling of (VI) with 3-chloro-N,N'-dimethylpropylamine (VII) by means of Williamson's reaction using NaH and NaI in refluxing DMF or using K2CO3 and HMPA in refluxing acetone.

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