【药物名称】
化学结构式(Chemical Structure):
参考文献No.610081
标题:N-acyl-1,2,3,4a,5,10b-hexahydro-[1]benzopyrano-[3,4-b][1,4]oxazine-9-carbonitriles as bladder-selective potassium channel openers
作者:Chiu, H.-I.; Lin, Y.-C.; Cheng, C.-Y.; Tsai, M.-C.; Yu, H.-C.
来源:Bioorg Med Chem 2001,9(2),383
合成路线图解说明:

Ring opening of the chiral epoxide (I) with 2-aminoethanol gave the trans-aminoalcohol (II). Subsequent intramolecular cyclization of (II) under Mitsunobu conditions afforded the chromenooxazine tricyclic system (III). The NH group of (III) was then acylated with anisoyl chloride (IV), yielding amide (V). This compound underwent epimerization at the C-10b position upon treatment with NaH to produce the more stable cis-fused isomer (VI). The methyl ether group of (VI) was finally cleaved by treatment with boron tribromide to furnish the corresponding phenol.

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