【药物名称】LB-30812
化学结构式(Chemical Structure):
参考文献No.668143
标题:Noncovalent tripeptidic thrombin inhibitors incorporating amidrazone, amine and amidine functions at P1
作者:Lee, K.; Jung, W.-H.; Park, C.W.; Park, H.D.; Lee, S.H.; Kwon, O.H.
来源:Bioorg Med Chem Lett 2002,12(7),1017
合成路线图解说明:

The N-protected dipeptide (I) is coupled to 4-(aminomethyl)benzonitrile (II) by means of EDC to afford amide (III). Acidic cleavage of the N-Boc group of (III) yields the deprotected amine (IV), which is then condensed with sulfamoyl chloride, producing sulfamide (V). From this, the target amidine can be obtained in two ways. Addition of hydrogen sulfide to the cyano group of (V), followed by S-alkylation with iodomethane, gives rise to the thioimidate (VI), which is then displaced with ammonium acetate to provide the desired amidine. Alternatively, addition of hydroxylamine to nitrile (V) leads to the amidoxime (VII) which, upon catalytic hydrogenation, is converted into the title amidine.

Drug Information Express,Drug R&D,Chemical Database,Patent Search.
Copyright © 2006-2024 Drug Future. All rights reserved.Contact Us