【药物名称】
化学结构式(Chemical Structure):
参考文献No.681694
标题:Synthesis and chemical characterization of 2-methoxy-N10-substituted acridones needed to reverse vinblastine resistance in multidrug resistant (MDR) cancer cells
作者:Krishnegowda, G.; Thimmaiah, P.; Hegde, R.; Dass, C.; Houghton, P.J.; Thimmaiah, K.N.
来源:Bioorg Med Chem 2002,10(7),2367
合成路线图解说明:

Ullmann condensation between o-chlorobenzoic acid (I) and p-anisidine (II) produces the diphenylamine carboxylic acid (III), which is further cyclized to the 2-methoxyacridone (IV) by heating in polyphosphoric acid. N-Alkylation of acridone (IV) with 1-bromo-4-chlorobutane (V) in the presence of KOH under phase-transfer conditions furnishes the N-(chlorobutyl)acridone (VI). Finally, nucleophilic substitution of the chloro group of (VI) with N-(2-hydroxyethyl)piperazine (VII) gives rise to the title compound.

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